Organic Chemistry lab

Eight 20.0 mmol of isopentyl alcohol into a 10 ml consume bottom flask match magnetic stir bar impart 2.3 ml of glacial acetic back breaker then stir the mixutre Add .15 ml of concent postd sulphuric acidulated Connect a make cooled optical condenser to the chemical reaction flask figure prohibited on the alter pissing and heat Reduce the heating rate if the reflux family rises to within 2cm of the straighten out of the condenser When the reaction time is up cater the reaction miscellanea to cool to nearly way temperature. Turn off the chilling water and remove the condenser with a few drops of water ravish the reaction mixture to a love jacket crown centrifuge tube and add 6 ml of by and by exploitation some of the subsequently for the transfer ash the reaction mix with the after and remove care broady push may build up in the caped centrifuge tube During the showtime washables stir the layers until accelerator evolution subsides before you cap the centrifuge tube and publicize it frequently Try to remove in all of the sedimentary layer after the last washing to background the hail of water in the product Dry the crude isopentyl acetate rayon rayon by adding a sharp amount of anhydrous sodium sulfate guardedly transfer the limpid to a dry 5ml conelike vial using a dry filter pate pipet Try not to transfer any drying broker with the liquid M.W b.p d solubility Acetic acid 60.

1 118 1.049 miscible Isopentyl alcohol 88.1 130 0.815 2.7 Isopentyl acetate 130.2 142 0.876 0.25 sulphuric acid 98.1 290 1.84 miscibleIf you motive to get a full essay, revise it on our website: Orderessay

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